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Herein, a photocatalytic acceptorless dehydrogenative aromatization of cyclohexanones or cyclohexenones at room temperature has been developed. The reaction features the visible-light and cobalt co-catalyzed sequential dehydrogenation of in-situ formed enol silyl ethers, enables a general and straightforward method for the synthesis of a series of phenols with diverse substitution patterns from cyclohexanones or cyclohexenones.
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