Crystallograpy
By using the Rigaku Oxford XCalibur diffractometer including EOS CCD
detector with MoKα radiation (λ = 0.7107 Ǻ) at room
temperature, the single crystallographic datas of two pyrazole
derivatives were obtained. CrysAlisPro software
package was utilised to perform data collections, cell refinements, data
reductions and absorption corrections [49]. Structure solution and
refinement process for both compounds were analysed by considering
direct methods with SHELXT and SHELXL respectively in OLEX2 software
[50–52]. All atoms except the hydrogen atoms were taken into
account as an anisotropic thermal elipsoids. The riding model was used
to determine the positions of hydrogen atoms. Crystallographic data of
both molecules are offered in Table 1.
Table 1 . Crystallographic details for the molecules.